Ultrasonic wave effects on the diameter of TiO2 nanoparticles

South African Journal of Science

 
 
Field Value
 
Title Ultrasonic wave effects on the diameter of TiO2 nanoparticles
 
Creator Milani Moghaddam, Hossain Nasirian, Shahruz
 
Subject Physics anatase; diameter; TiCl4; TiO2 nanoparticles; sol-gel method; ultrasound
Description Titanium dioxide (TiO2) nanostructured materials have attracted a great deal of attention because of their numerous applications. However, TiO2 applications depend strongly on the material’s high homogeneity and definite phase composition, morphology, particle size, high surface area and porosity, which are dependent on the sample history, the method of preparation and heat treatment. We synthesised TiO2 nanopowder with an anatase structure by the sol-gel method using TiCl4-ethanol solution as a precursor in an argon gas environment, with and without applying ultrasonic waves. Our results show that the use of ultrasonic waves (after aging) has a significant effect on the homogeneity and size of TiO2 nanoparticles. A smaller crystallite size was obtained using ultrasonic waves. For this purpose, the average diameter of TiO2 nanoparticles was decreased by about 3 nm. The synthesised powder was characterised by X-ray diffraction, scanning electron microscopy and transmission electron microscopy.
 
Publisher AOSIS
 
Contributor mazandaran university
Date 2011-03-14
 
Type info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion — sol-gel
Format application/pdf text/html text/xml
Identifier 10.4102/sajs.v107i3/4.389
 
Source South African Journal of Science; Vol 107, No 3/4 (2011); 5 pages 1996-7489 0038-2353
 
Language eng
 
Relation
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https://journals.sajs.aosis.co.za/index.php/sajs/article/view/389/587 https://journals.sajs.aosis.co.za/index.php/sajs/article/view/389/606 https://journals.sajs.aosis.co.za/index.php/sajs/article/view/389/609 https://journals.sajs.aosis.co.za/index.php/sajs/article/downloadSuppFile/389/1725 https://journals.sajs.aosis.co.za/index.php/sajs/article/downloadSuppFile/389/1726 https://journals.sajs.aosis.co.za/index.php/sajs/article/downloadSuppFile/389/1727 https://journals.sajs.aosis.co.za/index.php/sajs/article/downloadSuppFile/389/1728 https://journals.sajs.aosis.co.za/index.php/sajs/article/downloadSuppFile/389/1729 https://journals.sajs.aosis.co.za/index.php/sajs/article/downloadSuppFile/389/1730 https://journals.sajs.aosis.co.za/index.php/sajs/article/downloadSuppFile/389/1731
 
Coverage — — diameter of nanoparticles
Rights Copyright (c) 2011 Hossain Milani Moghaddam, Shahruz Nasirian https://creativecommons.org/licenses/by/4.0
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